HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Acetylphenylboronic acid → HCID 69291037, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Acetylphenylboronic acid | HCID 2734309 | — |
| Reactant | 6-Acetyl-3-fluoro-5,6-dihydro-2-(6-methoxy-3-pyridinyl)-pyrido[3,2-c][1]benzazocine | HCID 69291197 | — |
| Reactant | 1-(2-chloro-12H-1,11-diaza-dibenzo[a,e]cycloocten-11-yl)-ethanone | HCID 72366779 | — |
| Product | HCID 69291037 | HCID 69291037 | 92% |
Reaction Steps
The title compound (6.1 mg, 92%) was prepared from 55C (5.0 mg, 0.018 mmol) and 2-acetylphenylboronic acid (2.9 mg, 0.018 mmol) by a route analogous to that used for the preparation of 2B. HPLC Rt=2.363 min; LCMS Found: (M+H)+=369.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378426B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-d441e7c41b4049b8bc6f34d1ba0e46dc |
| Source note | uspto-grants-2008_05 |