3-Nitrobenzenesulfonyl chloride → HCID 69286981, compound
Reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([S:10](Cl)(=[O:12])=[O:11])[CH:7]=[CH:8][CH:9]=1)([O-])=O.[NH:14]1[CH2:20][CH2:19][CH2:18][C@H:15]1[CH2:16][OH:17]>>[NH2:1][C:4]1[CH:5]=[C:6]([S:10]([N:14]2[CH2:20][CH2:19][CH2:18][C@H:15]2[CH2:16][OH:17])(=[O:12])=[O:11])[CH:7]=[CH:8][CH:9]=1Participants
3
Procedure
By subjecting 3-nitro-benzenesulfonyl chloride and L-prolinol in analogous manner to the procedure described in example B.13, the title compound was obtained. Pale-yellow oil. MS (ISP) 257.3 [(M+H)+].
Sources & evidence
- ORD record
- ord-054c3d7c48bf4df3b0bd5a80b54ab815
- Source dataset
- uspto-grants-2008_05
- Patent number
- US07378417B2
Reaction notes
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