Benzenesulfonamide, 3-amino- → HCID 69292982, compound

HRID 2224541Notes

Reaction equation

HRID 2224541 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:13]=[CH:12][N:11]3[N:14]=[CH:15][C:16]([C:17]([OH:19])=O)=[C:10]3[N:9]=2)=[CH:4][CH:3]=1.[NH2:20][C:21]1[CH:22]=[C:23]([S:27]([NH2:30])(=[O:29])=[O:28])[CH:24]=[CH:25][CH:26]=1>>[S:27]([C:23]1[CH:22]=[C:21]([NH:20][C:17]([C:16]2[CH:15]=[N:14][N:11]3[CH:12]=[CH:13][C:8]([C:5]4[CH:4]=[CH:3][C:2]([Cl:1])=[CH:7][CH:6]=4)=[N:9][C:10]=23)=[O:19])[CH:26]=[CH:25][CH:24]=1)(=[O:28])(=[O:29])[NH2:30]

Participants

3

Reactant 2

HCID 7377Benzenesulfonamide, 3-amino-HCID 66650561HCID 66650561, compound

Product 1

HCID 69292982HCID 69292982, compound

Procedure

The title compound was prepared from 5-(4-chloro-phenyl)-pyrazolo[1,5-a]pyrimidine-3-carboxylic acid (example C.22) and 3-amino-benzenesulfonamide according to general procedure II. Pale-yellow solid. MS (ISP) 428.3 [(M+H)+]; mp 345° C.

Sources & evidence

ORD record
ord-f52b8f93eabb4f59bff0dd5abed4652d
Source dataset
uspto-grants-2008_05
Patent number
US07378417B2

Reaction notes

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