Benzenesulfonamide, 3-amino- → HCID 69292988, compound

HRID 2224547Notes

Reaction equation

HRID 2224547 reaction equation
[CH3:1][C:2]1[N:7]2[N:8]=[CH:9][C:10]([C:11]([OH:13])=O)=[C:6]2[N:5]=[C:4]([C:14]2[CH:19]=[CH:18][C:17]([C:20]([F:23])([F:22])[F:21])=[CH:16][CH:15]=2)[CH:3]=1.[NH2:24][C:25]1[CH:26]=[C:27]([S:31]([NH2:34])(=[O:33])=[O:32])[CH:28]=[CH:29][CH:30]=1>>[S:31]([C:27]1[CH:26]=[C:25]([NH:24][C:11]([C:10]2[CH:9]=[N:8][N:7]3[C:2]([CH3:1])=[CH:3][C:4]([C:14]4[CH:15]=[CH:16][C:17]([C:20]([F:22])([F:23])[F:21])=[CH:18][CH:19]=4)=[N:5][C:6]=23)=[O:13])[CH:30]=[CH:29][CH:28]=1)(=[O:32])(=[O:33])[NH2:34]

Participants

3

Reactant 2

HCID 7377Benzenesulfonamide, 3-amino-HCID 66650358HCID 66650358, compound

Product 1

HCID 69292988HCID 69292988, compound

Procedure

The title compound was prepared from 7-methyl-5-(4-trifluoromethyl-phenyl)-pyrazolo[1,5-a]pyrimidine-3-carboxylic acid (example C.25) and 3-amino-benzenesulfonamide according to general procedure II. Pale-yellow solid. MS (ISP) 476.5 [(M+H)+]; mp 270-272° C.

Sources & evidence

ORD record
ord-36fd28cc4c6145ea9523ff8c6123992d
Source dataset
uspto-grants-2008_05
Patent number
US07378417B2

Reaction notes

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