HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloride → HCID 16110249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloride | HCID 312 | — |
| Reactant | (4-Benzylpiperidin-1-yl)oxoacetic acid | HCID 16110264 | — |
| Product | HCID 16110249 | HCID 16110249 | 99.5% |
Reaction Steps
A mixture of 26.2 g (106 mmol) of (4-benzylpiperidin-1-yl)oxoacetic acid and 50 ml of thinyl chloride is refluxed for 2 h, then cooled and concentrated to yield 28.0 g (99.5%) of the title compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378431B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-c48cd70ec09248a192cd6800b6220432 |
| Source note | uspto-grants-2008_05 |