Ethyl 4,4-dibutyl-1-hydroxy-3-oxo-3,4-dihydro-2-naphthalenecarboxylate → 4-hydroxy-1,1-bis(3-methylbutyl)naphthalen-2(1H)-one

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Reaction Steps

The title compound was prepared according the procedure of Example 5B, substituting the product of Example 6F for the product of Example 4F. 1H NMR (300 MHz, CDCl3): δ 0.44 (m, 2 H) 0.73 (m, 14 H) 1.32 (m, 2 H) 1.94 (m, 2 H) 2.30 (m, 2 H) 7.49 (t, J=7.54 Hz, 2 H) 7.72 (m, 1 H) 8.26 (m, 1 H) 15.77, 15.72 (two s, 1 H).

Provenance & Evidence