HCID 68872644, compound → HCID 69268926, compound

HRID 2224808Notes

Reaction equation

HRID 2224808 reaction equation
[CH2:1]([C:5]([C:23]1[CH:28]=[CH:27][C:26]([F:29])=[CH:25][CH:24]=1)([CH2:19][CH2:20][CH2:21][CH3:22])[C:6]([CH:8](C(OCC)=O)[C:9]([O:11]CC)=O)=[O:7])[CH2:2][CH2:3][CH3:4].FC1C=CC(C(CCC)(CCC)C(C(C(OCC)=O)C(OCC)=O)=O)=CC=1>>[CH2:19]([C:5]1([CH2:1][CH2:2][CH2:3][CH3:4])[C:23]2[C:28](=[CH:27][C:26]([F:29])=[CH:25][CH:24]=2)[C:9]([OH:11])=[CH:8][C:6]1=[O:7])[CH2:20][CH2:21][CH3:22]

Participants

3

Reactant 2

HCID 68872644HCID 68872644, compoundHCID 68874303HCID 68874303, compound

Product 1

HCID 69268926HCID 69268926, compound

Procedure

The title compound was prepared according to the procedure of Example 14G, substituting the compound of Example 18E for the compound of Example 14F. 1H NMR (300 MHz, CDCl3): δ 0.52 (m, 2 H) 0.68 (t, J=7.35 Hz, 6 H) 0.88 (m, 2 H) 1.09 (m, 4 H) 1.82 (m, 2 H) 2.23 (m, 2 H) 6.17 (s, 1 H) 7.27 (m, 1 H) 7.42 (m, 1 H) 7.80 (dd, J=9.38, 2.76 Hz, 1 H).

Sources & evidence

ORD record
ord-e7477a0912ac4c72a55ef7b9447b0b74
Source dataset
uspto-grants-2008_05
Patent number
US07378414B2

Reaction notes

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