Sodium Hydroxide → HCID 44456254, compound

Participants

Reaction Conditions

Reaction Steps

A suspension of the product of Example 38C (0.339 g) in water (10 mL) was treated with 0.997N sodium hydroxide solution (0.595 mL, 0.593 mmol) and stirred at 25° C. for 1 hour. The solution was lyophilized to give the title compound (0.334 g, 95%). 1H NMR (300 MHz, DMSO-d6): δ ppm 0.63 m, 3 H) 0.98 m, 8 H) 1.45 m, 7 H) 1.68 m, 1 H) 2.09 m, 1 H) 2.93 m, 3 H) 7.30 m, 3 H) 7.45 m, 3 H) 8.05 m, 1 H) 9.87 m, 1 H) 15.45 m, 1 H). MS (ESI−) m/z 570 (M−H)−.

Provenance & Evidence