HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 69284652, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 69286639 | HCID 69286639 | — |
| Product | HCID 69284652 | HCID 69284652 | 55.3% |
Reaction Steps
Following the procedure of Example 7e, methyl 3-(2-((1R,2S,5R)-5-(ethyl(methyl)amino)-2-(2-(3-(trifluoromethyl)benzamido)acetamido)cyclohexyl)ethyl)benzoate (13 mg) was converted to the trifluoroacetic acid salt of the title compound as a white powder (7 mg) after purification by reverse phase HPLC and lyophilization. MS found: (M+H)+=534.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07378409B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-4a9cd3bee39a46779dc9808795efa762 |
| Source note | uspto-grants-2008_05 |