HCID 69285761, compound → HCID 131726908, compound

Participants

Reaction Steps

(1R,3R,4S)-(4-Benzyloxycarbonylamino-3-(methyl)sulfonylmethylcyclohexyl)carbamic acid tert-butyl ester (300 mg) was dissolved in MeOH (5 ml) prior to the addition of 10% Pd/C (200 mg). A hydrogen balloon was added and the solution was stirred for 3 h. The palladium was filtered off and the solution was concentrated to give tert-butyl(1R,3R,4S)-4-amino-3-(methylsulfonylmethyl)cyclohexylcarbamate (201 mg). MS found: (M+H)+307.2.

Provenance & Evidence