HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → Methyl 2-(4-hydroxymethylphenoxy)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | Methyl 2-(4-formylphenoxy)propanoate | HCID 18981016 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 2-(4-hydroxymethylphenoxy)propionate | HCID 18759642 | 83.1% |
Reaction Steps
By the method of Example 1, Step G, 11.1 g (0.0533 mole) of methyl 2-(4-formylphenoxy)propionate and 2.02 g (0.0533 mole) of sodium borohydride were reacted in methanol, yielding 9.31 g of methyl 2-(4-hydroxymethylphenoxy)propionate as a yellow oil. The NMR spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344812 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-df2872459a974f899b66e6939426e277 |
| Source note | uspto-grants-1994_09 |