HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → N-cyclohexyl-4-acetoxy-3-methoxycinnamamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | 4-Acetoxy-3-methoxycinnamoyl chloride | HCID 54468022 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | N-cyclohexyl-4-acetoxy-3-methoxycinnamamide | HCID 54552956 | — |
Reaction Steps
Using 3 g of 4-acetoxy-3-methoxycinnamoyl chloride, 1.4 ml of cyclohexylamine, and 100 ml of pyridine, a reaction similar to that conducted in Example 53 was carried out. As a result, 2.64 g of N-cyclohexyl-4-acetoxy-3-methoxycinnamamide (a compound of the present invention) was obtained as white crystal, which had the following physiochemical properties:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344845 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-ca199c655f08451b855bb274ad7df29f |
| Source note | uspto-grants-1994_09 |