4,4-Dimethylcyclohexan-1-amine → N-(4,4-dimethylcyclohexyl)-4-acetoxy-3-methoxycinnamamide

Participants

Reaction Steps

Using 8.9 g of 4-acetoxy-3-methoxycinnamoyl chloride, 3.81 g of 4,4-dimethyl-1-cyclohexylamine, and 100 ml of pyridine, a reaction similar to that conducted in Example 53 was carried out. As a result, 8.99 g of N-(4,4-dimethylcyclohexyl)-4-acetoxy-3-methoxycinnamamide (a compound of the present invention) was obtained as white crystal, which had the following physiochemical properties:

Provenance & Evidence