cis-4-Methylcyclohexylammonium chloride → HCID 178461400, compound

HRID 2225518Notes

Reaction equation

HRID 2225518 reaction equation
[Cl-:1].[CH3:2][CH:3]1[CH2:8][CH2:7][CH:6]([NH3+:9])[CH2:5][CH2:4]1>C(Cl)Cl>[Cl-:1].[CH3:2][C@H:3]1[CH2:8][CH2:7][C@H:6]([NH3+:9])[CH2:5][CH2:4]1

Participants

3

Reactant 1

HCID 45925625cis-4-Methylcyclohexylammonium chloride

Product 1

HCID 178461400HCID 178461400, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

4-methylcyclohexylammonium chloride (Example 71) was suspended in 4 ml of methylene chloride cooled. The crystal obtained was filtered out, yielding 3.2 g of trans-4-methylcyclohexylammonium chloride as white crystal, which had the following physiochemical properties:

Workup

  1. temperaturecooled
  2. customThe crystal obtained
  3. filtrationwas filtered out

Sources & evidence

ORD record
ord-a8cc399b69e8417d9d90b9d15e0ce362
Source dataset
uspto-grants-1994_09
Patent number
US05344845

Reaction notes

Loading…