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HRID2225518

反应详情

EQUATION

反应方程式

HRID 2225518 的结构方程式

REACTANTS

反应物

1
结构：CC1CCC([NH3+])CC1.[Cl-]
HCID45925625

未命名化合物

PRODUCTS

生成物

1
结构：C[C@H]1CC[C@H]([NH3+])CC1.[Cl-]
HCID178461400

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

4-methylcyclohexylammonium chloride (Example 71) was suspended in 4 ml of methylene chloride cooled. The crystal obtained was filtered out, yielding 3.2 g of trans-4-methylcyclohexylammonium chloride as white crystal, which had the following physiochemical properties:

WORKUP

后处理

  1. temperaturecooled
  2. customThe crystal obtained
  3. filtrationwas filtered out