HRID2225546

反应详情

EQUATION

反应方程式

HRID 2225546 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Using 4.8 g of N-(cis-4-methylcyclohexyl)-2-dimethylaminoacetamide (Example 109), 1.8 g of lithium aluminum hydride, 150 ml of THF, and 5 g of sodium sulfate decahydrate, a reaction similar to that performed in Example 78 was carried out. As a result, 2.9 g of N-(2-dimethylaminoethyl)-cis-4-methylcyclohexylamine was obtained as a colorless oil, which had the following physiochemical properties:

WORKUP

后处理

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