化工社化工社 化学情報印刷レポート · 研究参考用
HCID 178490509、化合物 → HCID 178490511、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | HCID 178490509 | HCID 178490509 | — |
| 触媒 | HCID 178418390 | HCID 178418390 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | HCID 178490511 | HCID 178490511 | 90.5% |
反応手順
Using a solution of 1 g of N-(2-dimethylaminoethyl)-N-(cis-4-methylcyclohexyl)-4-hydroxy-3-methoxycinnamamide (Example 111) in 60 ml of methanol, and 0.05 g of 10% palladium-carbon, a reaction similar to that conducted in Example 76 was carried out. As a result, 0.91 g of N-(2-dimethylaminoethyl)-N-(cis-4-methylcyclohexyl)-3-(4-hydroxy-3-methoxyphenyl)propionamide (a compound of the present invention) was obtained as a colorless oil, which had the following physiochemical properties:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05344845 |
| 出典データセット | uspto-grants-1994_09 |
| ORD ID | ord-7befdfd132924a2aa4dc697ab898de5c |
| 出典メモ | uspto-grants-1994_09 |