HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 178490515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178490553 | HCID 178490553 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178490515 | HCID 178490515 | 85.1% |
Reaction Steps
Using 3.7 g of N-(trans-4-methylcyclohexyl)-4-acetoxy-3-methoxycinnamamide (Example 130), 100 ml of methanol, and 5 g of potassium carbonate, a reaction similar to that conducted in Example 105 was carried out. As a result, 2.75 g of N-(trans-4-methylcyclohexyl)-4-hydroxy-3-methoxycinnamamide (a compound of the present invention) was obtained as white crystal, which had the following physiochemical properties:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344845 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-1f4b22497cae40868e9dc7a3cd02fbae |
| Source note | uspto-grants-1994_09 |