HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67757651, compound → HCID 67757641, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67757651 | HCID 67757651 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 67757641 | HCID 67757641 | 84% |
Reaction Steps
A mixture of (Z)-alpha-oxo-4-[(3-phenyl-2-propenyl)oxy]benzeneacetic acid methyl ester (1 g) in methanol (15 mL) and 0.5N sodium hydroxide (10 mL) was treated as in Example 19. Extraction provided solids which were crystallized from diethyl ether-hexane to give 0.8 g of colorless (Z)-alpha-oxo-4-[(3-phenyl-2-propenyl)oxy]benzeneacetic acid, mp 103°-105° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344843 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-caa4de766b9d4f3cbfcf8c925856f359 |
| Source note | uspto-grants-1994_09 |