HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54279774, compound → HCID 19004421, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54279774 | HCID 54279774 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 19004421 | HCID 19004421 | 91.8% |
Reaction Steps
A mixture of alpha-oxo-4-(2-phenoxyethoxy)benzeneacetic acid methyl ester (1.6 g) in methanol (10 mL) and 0.5N sodium hydroxide (30 mL) was treated as in Example 19. Extraction provided solids which were crystallized from diethyl ether-hexane to give 1.4 g of colorless alpha-oxo-4-[[2-(phenoxy)ethyl]oxy]benzeneacetic acid, mp 102°-103° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344843 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-f0c40757af7b42a892714f5b5e2619d4 |
| Source note | uspto-grants-1994_09 |