HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54335854, compound → 4-[[2-(4-Methylphenoxy)ethyl]oxy]-alpha-oxobenzeneacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54335854 | HCID 54335854 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | 4-[[2-(4-Methylphenoxy)ethyl]oxy]-alpha-oxobenzeneacetic acid | HCID 19004396 | 92.4% |
Reaction Steps
A mixture of 4-[[2-(4-methylphenoxy)ethyl]oxy]-alpha-oxobenzeneacetic acid methyl ester (0.68 g) in methanol and 0.5N sodium hydroxide (8 mL) was treated as in Example 19. Extraction provided solids which were crystallized from diethyl ether-hexane to give 0.6 g of colorless 4-[[2-(4-methylphenoxy)ethyl]oxy]-alpha-oxobenzeneacetic acid, mp 135-136° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344843 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-b2c88a86593f454a88b06a1703711f75 |
| Source note | uspto-grants-1994_09 |