Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2225978Generated: November 2, 2026

Water → HCID 70061333, compound

https://huagongshe.com/reaction/2225978

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantTriphenylphosphineHCID 11776—
ReactantHCID 131718659HCID 131718659—
SolventTetrahydrofuranHCID 8028—
ProductHCID 70061333HCID 70061333—

Reaction Steps

The title compound can be prepared by treating the title compound of Example 85 with triphenylphosphine and water in THF as described in the literature [N. Knouzi, M. Vaultier, R. Carrie Bull. of Chem. Soc. France, 815 (1985)] which can afford the title compound directly. The product can be purified by reverse phase HPLC using the conditions of Example 1 to afford the title compound. The product can be verified by C NMR.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05344957
Source datasetuspto-grants-1994_09
ORD IDord-d59c1577c9844a0385133e2c323ab3fd
Source noteuspto-grants-1994_09