HCID 19004149, compound → HCID 54517785, compound

Participants

Reaction Steps

A solution of 89 mg (0.11 mmole) of 2-(2-(N-(benzyloxycarbonyl)-N-(carbamoylmethyl)amino)-N-(methyl)ethylaminocarbonyl)-4-(N,N-di-n-pentylcarbamoyl)-1-(N-(3-chlorophenyl)-N-phenylcarbamoyl)piperazine in 6 mL of ethanol was treated with 50 mg of 10% Pd/C, and the resulting suspension was stirred under an atmosphere of hydrogen for 25 min. The mixture was then filtered through Celite and the filtrate concentrated in vacuo. The residue was carried on in Step F below.

Provenance & Evidence