HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → N-(3,5-Dichlorophenyl)-N-phenylcarbamoylchloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | 3,5-Dichloro-N-phenylaniline | HCID 19004131 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-(3,5-Dichlorophenyl)-N-phenylcarbamoylchloride | HCID 19004108 | — |
Reaction Steps
According to the procedure of Example 10, Step C, 10g (27.9 mmole) of N-(3,5-dichlorophenyl)aniline, 42 mL of 1.93M phosgene in toluene and 25 mL of toluene at a bath temperature of 105° C. for 4.5 hr gave 10.98 g of a yellow oil, which by 1H NMR was 40 mol % (46 wt %) product, the remainder being starting material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344830 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-448f6bda15324d30bf1b90dbe17a5f0d |
| Source note | uspto-grants-1994_09 |