HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl iodide → HCID 67940172, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl iodide | HCID 6362 | — |
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | HCID 67635404 | HCID 67635404 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 67940172 | HCID 67940172 | — |
Reaction Steps
The compound (74) (1.68 g) was esterified in the conventional procedure with 1,8-diazabicyclo[5.4.0]-7-undecene (DBU, 0.78 ml) and isopropyl iodide (0.35 ml) in acetonitrile (15 ml). The residue was subjected to silicagel column chromatography to give the titled compound (75). Yield: 0.908 g (88%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05346921 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-8645ef9ca5c542618e7e0de082da6c95 |
| Source note | uspto-grants-1994_09 |