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HRID2226407

反应详情

EQUATION

反应方程式

HRID 2226407 的结构方程式

REACTANTS

反应物

3
结构：O=C(O)CNC(=O)OCc1ccccc1
HCID14349

Glycine, N-[(phenylmethoxy)carbonyl]-

C10H11NO4

结构：CCOC(=O)[C@@H]1CC2(CN1)SCCS2
HCID14515252

未命名化合物

结构：CCOC(=O)[C@@H]1CC2(CN1C(=O)OCc1ccccc1)SCCS2
HCID14540988

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)[C@@H]1CC2(CN1C(=O)CNC(=O)OCc1ccccc1)SCCS2
HCID13373629

未命名化合物

PROCEDURE

实验过程

Convert 2.22 g of 7-benzyloxycarbonyl-1,4-dithia-7-azaspiro[4.4]nonane-8(S)-carboxylic acid, ethyl ester (prepared as described in paragraph A) to 1,4-dithia-7-azaspiro-[4.4]nonane-8(S)-carboxylic acid, ethyl ester as described in Example 23 and couple this compound with 1.5 g of N-benzyloxycarbonylglycine, N-hydroxysuccinimide ester as described in Example 23 to yield 7-(N-benzyloxycarbonylglycyl)-1,4-dithia-7-azaspiro[4.4]nonane-8(S)-carboxylic acid, ethyl ester, a yellow oil [α]D26 -21.0°.