HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-carbobenzyloxyalanine → HCID 131718676, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-carbobenzyloxyalanine | HCID 736104 | — |
| Reactant | HCID 18964777 | HCID 18964777 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 131718676 | HCID 131718676 | — |
Reaction Steps
To a solution of 9.4 g of ethyl azacyclooctane-2-carboxylate in 400 ml of ethyl acetate add 17.0 g of N-benzyloxycarbonyl- (S) -alanine, N-hydroxysuccinimide ester. Stir the reaction mixture at room temperature for 20 hours and concentrate it in vacuo to give 1-[N-benzyloxycarbonyl-(S)-alanyl]azacyclooctane-2(R,S)-carboxylic acid, ethyl ester, as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05348944 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-2a5bd89b6e5c4d64a10d8e38803713de |
| Source note | uspto-grants-1994_09 |