HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → N-(3-methylphenyl)-N-phenylcarbamoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | N-(3-Methylphenyl)aniline | HCID 14569 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-(3-methylphenyl)-N-phenylcarbamoyl chloride | HCID 18965178 | 100% |
Reaction Steps
According to the procedure of Example 15, Step A, 3.66 g (20 mmole) of 3-methyldiphenylamine, 20 mL (38.6 mmole) of 1.93M phosgene is toluene solution, and 20 mL of toluene gave 4.9 g (100%) of a dark solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05348955 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-a3cdeb12b964452fb5d818efe11793f1 |
| Source note | uspto-grants-1994_09 |