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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2226635Generated: October 31, 2026

Benzyl Alcohol → HCID 10903965, compound

https://huagongshe.com/reaction/2226635

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzyl AlcoholHCID 244—
ReactantPyridineHCID 1049—
Reactant4-Toluenesulfonyl chlorideHCID 7397—
SolventAcetoneHCID 180—
ProductHCID 10903965HCID 1090396580%

Reaction Conditions

Temperature5 °C

Reaction Steps

19.07 g (0.1 mol) of tosyl chloride and 15.82 g (0.2 mol) of pyridine were dissolved in 60 g of acetone, and, after cooling to 5° C., there was added 10.81 g (0.1 mol) of benzyl alcohol. While suppressing excessive elevation of the temperature, reaction was allowed for 5 hours. After the completion of the reaction, the mixture was concentrated and the precipitated white solid was washed with ether and dried to give N-benzylpyridinium tosylate. Yield: 80%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05349067
Source datasetuspto-grants-1994_09
ORD IDord-f046dce07e9f4d11925e7c60b21bc0c4
Source noteuspto-grants-1994_09