Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 10903965 | HCID 10903965 | 80% |
Reaction Steps
19.07 g (0.1 mol) of tosyl chloride and 15.82 g (0.2 mol) of pyridine were dissolved in 60 g of acetone, and, after cooling to 5° C., there was added 10.81 g (0.1 mol) of benzyl alcohol. While suppressing excessive elevation of the temperature, reaction was allowed for 5 hours. After the completion of the reaction, the mixture was concentrated and the precipitated white solid was washed with ether and dried to give N-benzylpyridinium tosylate. Yield: 80%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05349067 |
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| Source dataset | uspto-grants-1994_09 |
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| ORD ID | ord-f046dce07e9f4d11925e7c60b21bc0c4 |
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| Source note | uspto-grants-1994_09 |
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