Benzyl Alcohol → HCID 21910218, compound

Participants

Reaction Conditions

Reaction Steps

19.07 g (0.1 mol) of tosyl chloride, 12.12 g (0.1 mol) of N,N-dimethylaniline and 10.1 g (0.1 mol) of triethylamine were dissolved in 60 g of tetrahydrofuran, and, after cooling to 10° C., there was added 10.81 g (0.1 mol) of benzyl alcohol. While suppressing excessive elevation of the temperature, the reaction was allowed for 5 hours. After the completion of the reaction, the mixture was concentrated, and the precipitated white solid was washed with ether and dried to give N-benzyl-N,N-dimethylanilinium tosylate. Yield: 70%.

Provenance & Evidence