HCID 10903965, compound → HCID 22924283, compound

HRID 2226639Notes

Reaction equation

HRID 2226639 reaction equation
S(C1C=CC(C)=CC=1)([O-])(=O)=O.[CH2:12]([N+:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1.[F:25][Sb-:26]([F:31])([F:30])([F:29])([F:28])[F:27].[Na+]>O>[F:25][Sb-:26]([F:31])([F:30])([F:29])([F:28])[F:27].[CH2:12]([N+:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

4

Reactant 2

HCID 10903965HCID 10903965, compoundHCID 16689647Sodium hexafluoroantimonate

Product 1

HCID 22924283HCID 22924283, compoundYield 72%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

34.13 g (0.1 mol) of N-benzylpyridinium tosylate obtained in Example 1 was dissolved in 100 of water, and was added to 25.88 g (0.1 mol) of sodium hexafluoroantimonate. The precipitated while solid was washed with ether and dried to give the titled compound. Yield: 72%.

Workup

  1. customThe precipitated while solid
  2. washwas washed with ether
  3. customdried

Sources & evidence

ORD record
ord-fe283c62451a4af996aa22700980c600
Source dataset
uspto-grants-1994_09
Patent number
US05349067

Reaction notes

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