Aldoxime → HCID 19038320, compound

HRID 2226654Notes

Reaction equation

[CH:1](=[N:3][OH:4])[CH3:2].[CH3:5][C:6]1[CH:7]=[C:8]([C:25]2[N:29]=[C:28]([C:30]([F:33])([F:32])[F:31])[O:27][N:26]=2)[CH:9]=[C:10]([CH3:24])[C:11]=1[O:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][C:22]#[CH:23]>>[CH3:24][C:10]1[CH:9]=[C:8]([C:25]2[N:29]=[C:28]([C:30]([F:31])([F:33])[F:32])[O:27][N:26]=2)[CH:7]=[C:6]([CH3:5])[C:11]=1[O:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][C:22]1[O:4][N:3]=[C:1]([CH3:2])[CH:23]=1

Participants

Reactant 2

HCID 7863Aldoxime

HCID 19038304HCID 19038304, compound

Product 1

HCID 19038320HCID 19038320, compound

Procedure

Following Procedure 1 and using equivalent amounts of acetaldehyde oxime and 3-[3,5-dimethyl-4-(9-ethinylnonyloxy)phenyl]-5-trifluoromethyl-1,2,4-oxadiazole, there can be obtained 5-{9-[2,6-dimethyl-4-(5-trifluoromethyl-1,2,4-oxadiazol-3-yl)phenoxy]nonyl}-3-methylisoxazole [I; R1 =CH3, Y=(CH2)9, R2 and R3 =2,6-(CH3)2, R4 =CF3 ].

Sources & evidence

ORD record: ord-a226014eaf5b4cfd88829f2f39875e5c
Source dataset: uspto-grants-1994_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05349068

Reaction notes

Loading…