HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178462340, compound → HCID 178476377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178462340 | HCID 178462340 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Product | HCID 178476377 | HCID 178476377 | — |
Reaction Steps
150 mg of Z-Asn-Thr-Pro-Arg(NO2)-OBzl was reduced in the presence of palladium-carbon in the same manner as in Example 7-(4). The resulting product was purified by high-performance liquid chromatography at 12 ml/min. (flow rate), to 10 % (B) 20 min. linear gradient (A) (mobile phase), subjected to Dowex 1×2 (acetate type) treatment and freeze-dried to obtain the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05349050 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-d88f2248c86740bd97d50f6faf399343 |
| Source note | uspto-grants-1994_09 |