HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178462154, compound → HCID 178476376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178462154 | HCID 178462154 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Product | HCID 178476376 | HCID 178476376 | — |
Reaction Steps
150 mg of Z-Asn-Ala-Pro-Arg(NO2)-OBzl was reduced in the presence of palladium-carbon in the same manner as in Example 7-(4). The resulting product was purified by high-performance liquid chromatography at 12 ml/min. (flow rate), 0 to 10% (B) 20 rain, linear gradient (A) (mobile phase), subjected to Dowex 1×2 (acetate type) treatment and freeze-dried to obtain the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05349050 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-1ba5d6aa1dfc444e9292526fd61d2b4f |
| Source note | uspto-grants-1994_09 |