Nonan-5-ol → HCID 18963613, compound

HRID 2226799Notes

Reaction equation

HRID 2226799 reaction equation
[N:1]1[C:14]2[C:5](=[CH:6][CH:7]=[C:8]3[C:13]=2[N:12]=[CH:11][CH:10]=[CH:9]3)[C:4](C(Cl)=[O:16])=[CH:3][CH:2]=1.C(N(C)[C:31]([C:33]1[C:46]2[C:37](=[C:38]3[C:43](=[CH:44][CH:45]=2)[CH:42]=[CH:41][CH:40]=[N:39]3)[N:36]=[CH:35][CH:34]=1)=[O:32])CCCCCCCCCCC.[CH3:48][CH2:49][CH2:50][CH2:51][CH:52]([OH:57])[CH2:53][CH2:54][CH2:55][CH3:56]>N1C=CC=CC=1>[N:12]1[C:13]2[C:8](=[CH:7][CH:6]=[C:5]3[C:14]=2[N:1]=[CH:2][CH:3]=[CH:4]3)[CH:9]=[CH:10][C:11]=1[C:31]([O:57][CH:52]([CH2:53][CH2:54][CH2:55][CH3:56])[CH2:51][CH2:50][CH2:49][CH3:48])=[O:32].[CH2:48]([C:45]1[CH:44]=[C:43]2[C:38]([N:39]=[CH:40][CH:41]=[CH:42]2)=[C:37]2[C:46]=1[C:33]([C:31]([O-:32])=[O:16])=[CH:34][CH:35]=[N:36]2)[CH2:49][CH2:50][CH2:51][CH2:52][CH2:53][CH2:54][CH2:55][CH3:56]

Participants

6

Reactant 3

HCID 12202Nonan-5-olHCID 18963612HCID 18963612, compoundHCID 18963616HCID 18963616, compound

Product 2

HCID 18963613HCID 18963613, compoundHCID 67820428HCID 67820428, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

5-nonyl 1,10-phenanthroline carboxylate was synthesized as follows: 1 equivalent of 1,10-phenanthroline-4-carbonyl chloride (prepared as described above in the discussion of N-dodecyl-N-methy-1,10-phenanthroline-4-carboxamide) was reacted with 1 equivalent of 5-nonanol in the presence of pyridine to give the desired product, 5-nonyl-1,10-phenanthroline-4-carboxylate.

Sources & evidence

ORD record
ord-2de7fb43aef243618dc888876dbdece9
Source dataset
uspto-grants-1994_09
Patent number
US05350518

Reaction notes

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