HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dimethyl-3-pentanone → 2,4-Dimethyl-2-(4-methylbenzene-1-sulfonyl)pentan-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dimethyl-3-pentanone | HCID 11271 | — |
| Reactant | Bis(cyclohexylsulfonyl)diazomethane | HCID 11056751 | — |
| Reactant | HCID 11175590 | HCID 11175590 | — |
| Product | 2,4-Dimethyl-2-(4-methylbenzene-1-sulfonyl)pentan-3-one | HCID 21872575 | — |
Reaction Steps
Using diisopropylketone, the reaction was carried out in the same manner as described in Synthesis Example 9, (2) and (3). The crude solid was recrystallized from n-hexane/benzene to afford 2,4-dimethyl-2-(p-toluenesulfonyl)pentan-3-one as white leaflets.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05350660 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-ad062004169947d7a9e25826f3eaeedc |
| Source note | uspto-grants-1994_09 |