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HRID2226820

反应详情

EQUATION

反应方程式

HRID 2226820 的结构方程式

REACTANTS

反应物

3
结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：C[C@H](N)C(=O)N[C@@H](C)C(=O)O
HCID5484352

L-Alanyl-L-alanine

C6H12N2O3

结构：C[C@H](NC(=O)[C@@H](N)Cc1ccccc1)C(=O)O
HCID5488196

Phenylalanylalanine

C12H16N2O3

PRODUCTS

生成物

1
结构：C[C@H](NC(=O)[C@H](C)NC(=O)[C@H](C)NC(=O)[C@@H](N)Cc1ccccc1)C(=O)O
HCID131718680

未命名化合物

PROCEDURE

实验过程

0.2 ml of aqueous solution containing 2 mM Mal-Phe-Ala OEtCl, 50 mM H-Ala-Ala-OH, 25 mM NaOH and 0.15 mg/ml papain are deep-frozen. Subsequently the reaction mixture is kept at -25° C. until the Mal-Phe-Ala-OEtCl is consumed. Following thawing, the yield is determined analytically by RP-HPLC and amounts to 79% of theory.

WORKUP

后处理

  1. temperatureare deep-frozen
  2. customis consumed