HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxy-4-(3-hydroxy-trans-prop-1-enyl)tetrahydropyran → 3-(4-Methoxytetrahydropyran-4-yl)-trans-propenoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxy-4-(3-hydroxy-trans-prop-1-enyl)tetrahydropyran | HCID 15199064 | — |
| Reactant | Jones' reagent | HCID 131709961 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 3-(4-Methoxytetrahydropyran-4-yl)-trans-propenoic acid | HCID 67825144 | — |
Reaction Steps
4-(3-hydroxy-trans-prop-1-enyl)-4-methoxy-tetrahydropyran (175 mg, 1.02 mmol), prepared as in Example 1, steps 1-3, was oxidized to the corresponding carboxylic acid by treatment with a slight excess of Jones reagent in cold acetone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05350765 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-d1fc65eb1cca484ea7bd4cbe9566e24d |
| Source note | uspto-grants-1994_09 |