HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → 3-(3,4-Dimethoxyphenyl)propionic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | Veratraldehyde | HCID 8419 | — |
| Reactant | 2-Phenyl-1,3-dioxane-4,6-dione | HCID 933829 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 3-(3,4-Dimethoxyphenyl)propionic acid | HCID 75019 | — |
Reaction Steps
25 ml of the mixture of formic acid and triethylamine prepared as described in Example 1 were added to a mixture of 4.8 g (0.025 mol) of 2-phenyl-1,3-dioxane-4,6-dione (m.p.: 148° C.) and 4.15 g (0.025 mol) of veratraldehyde. The reaction was carried out according to Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05350872 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-53c4755b30c94dd4bdd836cf47741ffb |
| Source note | uspto-grants-1994_09 |