HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → 3-(3,4-Dimethoxyphenyl)propionic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | Veratraldehyde | HCID 8419 | — |
| Reactant | 2-(4-Fluorophenyl)-1,3-dioxane-4,6-dione | HCID 19938682 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 3-(3,4-Dimethoxyphenyl)propionic acid | HCID 75019 | — |
Reaction Steps
5.26 g (0.025 mol) of 2-(4-fluorophenyl)-1,3-dioxane-4,6-dione (m.p.: 166°-167° C.) and 4.15 g (0.025 mol) of veratraldehyde were added to 25 ml of the mixture of formic acid and triethylamine prepared as described in Example 1. The reaction was carried out according to Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05350872 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-93ad8b5c70aa4baeb0248dd498d8ee07 |
| Source note | uspto-grants-1994_09 |