HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dimethylpyridine → HCID 15030144, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dimethylpyridine | HCID 11565 | — |
| Reactant | N-[3-(Bromomethyl)phenyl]-4-(tetradecyloxy)-benzeneacetamide | HCID 10052253 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 15030144 | HCID 15030144 | 88.3% |
Reaction Steps
A mixture of 1.5 g of N-[3-(bromomethyl)phenyl]-4-(tetradecyloxy)benzeneacetamide and 933.5 mg of 3,5-lutidine is refluxed in 25 ml of acetonitrile for 4 hours under argon. The solvent is evaporated and the residue stirred with ether and collected by centrifugation. The solid is washed several times with ether and vacuum dried to give 1.6 g of the desired product as a white powder, m.p. 122°-125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05350759 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-b1aa55e6d1c045998c429d17bfd56e06 |
| Source note | uspto-grants-1994_09 |