HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromoaniline → HCID 11208672, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromoaniline | HCID 11562 | — |
| Reactant | Diethyl squarate | HCID 123228 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 11208672 | HCID 11208672 | — |
Reaction Steps
1.7 g of 3,4-diethoxy-3-cyclobuten-1,2-dione in 25 mL of absolute ethyl alcohol was added 1.7g of 3-bromoaniline, the reaction mixture was stirred at room temperature for 20 hours, then 0.4 g of 3-bromoaniline was added and the reaction mixture was stirred for 48 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06413996B2 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-9f308ade30c042cfb662734439d0a704 |
| Source note | uspto-grants-2002_07 |