Benzyl mercaptan → HCID 86588947, compound

Participants

Reaction Steps

A solution of 4-methylphenylacetylene (0.02 mol) and benzyl mercaptan (0.02 mol) and metallic sodium (0.02 g atom) was subjected to the General Procedure to form Z-4-methylstyryl benzylsulfide. The title compound was obtained in 70% yield following oxidation. 1HNMR (CDCl3) δ 2.48 (3H, s), 4.60 (2H, s), 6.68 (1H, d, JH,H=11.94), 7.20-7.65 (9H aromatic+1H ethylenic).

Provenance & Evidence