HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
7-(benzyloxy)-2,3,4,5-tetrahydro-1H-3-benzazepine → 7-[(2-Fluoro-4-iodophenyl)oxy]-2,3,4,5-tetrahydro-1H-3-benzazepine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 7-(benzyloxy)-2,3,4,5-tetrahydro-1H-3-benzazepine | HCID 57437617 | — |
| Edukt | 1,1-Dimethylethyl 7-[(2-fluoro-4-Iodophenyl)oxy]-1,2,4,5-tetrahydro-3H-3-benzazepine-3-carboxylate | HCID 58984572 | — |
| Produkt | 7-[(2-Fluoro-4-iodophenyl)oxy]-2,3,4,5-tetrahydro-1H-3-benzazepine | HCID 58984576 | — |
Reaktionsschritte
The title compound was prepared from 1,1-dimethylethyl 7-[(2-fluoro-4-iodophenyl)oxy]-1,2,4,5-tetrahydro-3H-3-benzazepine-3-carboxylate (E274, Step 3) using an analogous method to that described for Description 2 (D2). MS (ES+) m/e 384 [M+H]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08207331B2 |
| Quelldatensatz | uspto-grants-2012_06 |
| ORD ID | ord-a32a5ec8f7804c7c977a839c1f44fb63 |
| Quellennotiz | uspto-grants-2012_06 |