HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12132980, compound → HCID 12132981, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12132980 | HCID 12132980 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 12132981 | HCID 12132981 | 100% |
Reaction Steps
Following the procedure of method 1C, methyl (2S)-3-hydroxy-2-[(1,2,3,4-tetrahydrocyclopenta[b]indol-5-ylcarbonyl)amino]propanoate(8.9 mmol, 2.7 g) was hydrogenated using 5% Pd/C (2 g) and concentrated HCI (10 mL) in methanol (25 mL) to yield the crude product (8.9 mmol, 2.7 g, quantitative).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06414144B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-42a4d86cf2da4c64b15b1bfb59f9d4ab |
| Source note | uspto-grants-2002_07 |