HCID 3018486, compound → HCID 69584266, compound

HRID 2227784Notes

Reaction equation

HRID 2227784 reaction equation
[O:1]1[CH2:3][C@H:2]1[CH2:4][O:5][C:6]1[C:18]2[C:17]3[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=3)[NH:11][C:10]=2[CH:9]=[CH:8][CH:7]=1.NC(C)CC[C:23]1[CH:31]=[CH:30][C:26]([C:27]([NH2:29])=[O:28])=[CH:25][CH:24]=1>>[OH:1][C@@H:2]([CH2:3][N:11]([C:23]1[CH:24]=[CH:25][C:26]([C:27](=[O:28])[NH2:29])=[CH:30][CH:31]=1)[CH2:10][CH:18]([CH3:6])[CH3:17])[CH2:4][O:5][C:6]1[C:18]2[C:17]3[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=3)[NH:11][C:10]=2[CH:9]=[CH:8][CH:7]=1

Participants

3

Reactant 2

HCID 3018486HCID 3018486, compoundHCID 10879208(S)-(+)-4-(2,3-Epoxypropoxy)carbazole

Product 1

HCID 69584266HCID 69584266, compound

Procedure

Titled compound was prepared substantially in accordance with Example 114 from (S)-4-(oxiranylmethoxy)-9H-carbazole (0.479 g, 2 mmol) and 4-[3-amino-3-methylpropyl]benzamide (580 mg, 3mmol) to yield product after purification. MS(m+1) 432.

Workup

  1. customto yield product
  2. customafter purification

Sources & evidence

ORD record
ord-68c1d5b3bfa940ea91b44fca1c61f6a9
Source dataset
uspto-grants-2002_07
Patent number
US06413991B1

Reaction notes

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