HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18472333, compound → HCID 18472283, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18472333 | HCID 18472333 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18472283 | HCID 18472283 | 91% |
Reaction Steps
A mixture of (3-methoxypyridin-2-yl)—(4-nitro-phenyl)methanol (600 mg) and 5% Pd-C (0.06 g) in ethanol (20 ml) was vigorously stirred under hydrogen atmosphere for 3 hours, and the Pd-C was filtered off. The filtrate was concentrated under reduced pressure to give (4-amino-phenyl)—(3-methoxypyridin-2-yl)-methanol (483 mg) as pale yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06413947B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-61bc525cf6d04a8db36242d0ee60959d |
| Source note | uspto-grants-2002_07 |