HCID 54289398, compound → 1,1-Dimethylethyl 4-(methylamino)butanoate

Participants

Reaction Steps

In methanol (70 ml) was dissolved tert-butyl 4-[(benzyloxy)carbonyl]−4-methylaminobutyrate (6.06 g), and to the mixture was added 10% palladium-carbon (580 mg). Under hydrogen atmosphere, the mixture was stirred at room temperature for 3 hours, and 10% palladium-carbon was removed. The solvent was evaporated under reduced pressure to give tert-butyl 4-methylaminobutyrate (3.35 g, 98%).

Provenance & Evidence