HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 18469740, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Diphenylmethane | HCID 7580 | — |
| Reactant | Chlorosulfonic acid | HCID 24638 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18469740 | HCID 18469740 | — |
Reaction Steps
To 33.6 g (0.2 mol) of diphenylmethane in 100 g of dichloromethane at room temperature, 23.4 g (0.2 mol) of chlorosulfonic acid was added dropwise. The solution was ripened for 2 hours, whereupon 50 g of water was added. This reaction mixture was used in the subsequent reaction without isolation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06416928B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-2c34225c8a43443e9af71a852947c23d |
| Source note | uspto-grants-2002_07 |