HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromocyclopentane → 2-Cyclopentyloxy-3,4-dimethoxybenzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromocyclopentane | HCID 8728 | — |
| Reactant | 2-Hydroxy-3,4-dimethoxybenzonitrile | HCID 11994758 | — |
| Product | 2-Cyclopentyloxy-3,4-dimethoxybenzonitrile | HCID 18470646 | 95% |
Reaction Steps
The subtitle compound was prepared from 2-hydroxy-3,4-dimethoxybenzonitrile and freshly distilled cyclopentyl bromide following the procedure described in Example 10(d). The crude product was purified on silica gel eluting with dichloromethane to give the subtitle compound as a colourless oil (95%). Rf 0.50 (dichloromethane). MS m/z 265 (MNH4)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06417194B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-80b43739db624a9f8b64d556ab864f59 |
| Source note | uspto-grants-2002_07 |