HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromoaniline → N-(4-bromophenyl)-2-nitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromoaniline | HCID 7807 | — |
| Reactant | 1-Fluoro-2-nitrobenzene | HCID 73895 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | N-(4-bromophenyl)-2-nitroaniline | HCID 12000290 | — |
Reaction Steps
The product (6.49 g) is obtained according to the method of stage 1 of Example 4, by using 3.73 mL of 2-fluoro-nitrobenzene and 7.31 g of 4-bromoaniline in the presence of 6.36 g of potassium tert-butanolate in 120 mL of DMSO.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08207373B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-ff8b1bc6869c4847892cf242936975a7 |
| Source note | uspto-grants-2012_06 |